IR, 1H NMR: In the IR spectrum (SM 22.214.171.124) can be observed a broad absorption near 3400 cm-1 (O-H from water) ... Vanillin (4-hydroxy-3-methoxybenzaldehyde) has found many uses in organic chemistry teaching laboratories, there are many examples where vanillin features as values cannot be derived. Country of Origin is subject to change. An example of such a spectrum is that of the flavoring agent vanillin, shown below. The structure of the product had been confirmed that is consistent with the predicted result using the spectral data. However, NIST makes no warranties to that effect, and NIST HTML 5 canvas support. Follow the links above to find out more about the data such sites. Be sure you find specific evidence of stretching of all types of bonds that this structure contains, and also bending consistent with its aromatic substitution pattern (the label of that bending must include what the substitution pattern is). intended to imply recommendation or endorsement by the National For example, a C=N double bond is about twice as strong as a C-N single bond, and the CN triple bond is similarly stronger than the double bond. The infrared spectrum of vanillin shows a -C=O stretch for aromatic aldehyde and an aromatic -C-O stretch for an ether which are unique fingerprint regions for vanillin. The spectrum of vanillin shows this for the phenolic hydroxyl, which is hydrogen bonded to the adjacent ether oxygen. The hydrolysis of acetylsalicylic acid is reported to be fast in base. Notice: Concentration information is not Vanillin View entire compound with free spectra: 119 NMR, 11 FTIR, 3 Raman, 3 UV-Vis, and 37 MS. SpectraBase Compound ID ... Molecular Formula: C8H8O3: Exact Mass: 152.047344 g/mol: Transmission Infrared (IR) Spectrum. Note the two features of the spectrum — the C-H absorptions between 2,800 cm –1 to 3,000 cm … The lignin-based vanillin is the type made from wood pulp byproduct and has a richer flavor. Vanillin, NF is used as a flavoring agent in pharmaceutical formulations. Soluble in alcohol, chloroform, ether, propylene glycol at 50°C, 1 g dissolves in 5 ml of 95% ethanol. The chemicals used to produced vanillin give the product a vanilla taste by essentially tricking the brain into thinking it’s the real thing. Follow the links above to find out more about the data 3. OH 1. UV/VIS spectral data of vanillin-semicarbazone recorded in 95 % ethanol Figure 3. It is possible to acquire IR spectra of hydroxyl-containing compounds without seeing this broad signal. Ethyl Vanillin, also known as Ethylvanillin, is an organic compound which is used in the production of the chocolate as a flavorant. o-Vanillin has been used to study the solvent-free reaction between o-vanillin and p-toluidine using NMR, DSC and XRD analysis. Go To: Top, References, Notes Data compilation copyrightby the U.S. Secretary of Commerce on behalf of the U.S.A.All rights reserved. The are too many minor peaks, and most of the times it is impossible to identify ALL the peaks (especially at lower wavelength) in an IR, what is important is identifying the major FUNCTIONAL groups as … Furthermore, the compound did not melt at temperatures suggested … Your institution may already be a subscriber. All rights reserved. Detailed Information on Carbonyl IR: C=O: stretch: 1670-1820: strong (conjugation moves absorptions to lower wave numbers) Ether; C-O: stretch: 1000-1300 (1070-1150) strong: Nitrile CN: stretch: 2210-2260 medium: Nitro; N-O: stretch: 1515-1560 & 1345-1385 strong, two bands Go To: Top, Infrared Spectrum, References. 55. It has a strong and intense vanilla like smell. errors or omissions in the Database. The purpose of the fee is to recover costs associated Packaging 10, 100, 500 g in glass bottle Biochem/physiol Actions o-Vanillin induces DNA damage as … Table 1. Enter the desired X axis range In acidic condition. Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director.
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